Sodium Azide → HCID 11099148, compound

Participants

Reaction Steps

Sodium azide (2.3 g, 36.0 mmol) was added to a solution of Example 13F in DMF (30 mL). After stirring at room temperature overnight, the reaction mixture was diluted with EtOAc, washed with brine, dried (MgSO4), filtered and concentrated. The concentrate was purified by flash chromatography using hexanes/ethyl acetate (3/2) to afford 1.36 g (36%) of the desired product as a colorless oil.

Provenance & Evidence