HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Azide → HCID 91224768, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | HCID 131723975 | HCID 131723975 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 91224768 | HCID 91224768 | — |
Reaction Steps
Sodium azide can be added to a solution of Example 17G in DMF. The reaction mixture can be stirred overnight at room temperature, diluted with EtOAc, washed with brine, dried (MgSO4), filtered and concentrated. The concentrate can be purified by flash column chromatography to afford the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06593314B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-35bc4c9d9fba44b3b83511bdb6f520de |
| Source note | uspto-grants-2003_07 |