HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → Triphenylphosphine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Product | Triphenylphosphine | HCID 11776 | — |
| Product | HCID 86759065 | HCID 86759065 | — |
Reaction Steps
Triphenylphosphine can be slowly added to a solution of Example 13I in THF. The reaction mixture can be stirred for 2 hours at room temperature, then water and triethylamine are added. The reaction mixture can be stirred for an additional 10 hours, then the reaction mixture can be concentrated. The concentrate can be chromatographed to afford the desired product with Ph3P as a contaminant.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06593314B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-a76305a7542249f09801e0ad31e878c5 |
| Source note | uspto-grants-2003_07 |