HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Dichloropyrazine → HCID 18186804, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Dichloropyrazine | HCID 78504 | — |
| Reactant | 3-(Pyrrol-1-Yl)Thiophene-2-Methanol | HCID 342464 | — |
| Product | HCID 18186804 | HCID 18186804 | — |
Reaction Steps
The title compound was prepared according to the procedure of example 50, step 1, starting from 3-(pyrrol-1-yl)thiophene-2-methanol (2.5 g, 14 mmol), K-t-BuO (1.43 g, 12.7 mmol) and 2,6-dichloropyrazine (1.73 g, 11.6 mmol). The yield of the title compound was 3.05 g (90%) and was obtained as an oil. Anal. (C13H10ClN3OS) C, H, N.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06593330B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-236f45e8b7b84a00853d5cd7e885dab2 |
| Source note | uspto-grants-2003_07 |