HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Phenylmethoxy)benzenemethanol → 2-{[3-(Benzyloxy)Benzyl]Oxy}-6-Chloropyrazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Phenylmethoxy)benzenemethanol | HCID 74341 | — |
| Reactant | 2,6-Dichloropyrazine | HCID 78504 | — |
| Product | 2-{[3-(Benzyloxy)Benzyl]Oxy}-6-Chloropyrazine | HCID 18186928 | — |
Reaction Steps
The title compound was prepared according to the procedure of example 50, step 1, starting from 3-benzyloxybenzyl alcohol (3.46 g, 16.2 mmol), K-t-BuO (1.69 g, 15.1 mmol) and 2,6-dichloropyrazine (1.97 g, 13.2 mmol). The yield of the title compound was 2.64 g (61%) and was obtained as a semisolid. Anal. (C18H15ClN2O2) C, H, N.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06593330B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-f657dee9892e4e62ae6b81ae45bc7bac |
| Source note | uspto-grants-2003_07 |