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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1357750Generated: October 26, 2026

2,1,3-Benzothiadiazol-5-ylmethanol → 2,1,3-Benzothiadiazole-5-carbaldehyde

https://huagongshe.com/reaction/1357750

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2,1,3-Benzothiadiazol-5-ylmethanolHCID 2776294—
CatalystHCID 178418406HCID 178418406—
SolventChloroformHCID 6212—
Product2,1,3-Benzothiadiazole-5-carbaldehydeHCID 277629072.3%

Reaction Steps

5-Hydroxymethylbenzo-2, 1,3-thiadiazole (2.6 g, 16 mmol) and manganese dioxide (6.0 g, 64 mmol) in chloroform (150 mL) were stirred at room temperature overnight. The reaction mixture was filtered off and the filtrate was evaporated to provide 1.9 g of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06593335B1
Source datasetuspto-grants-2003_07
ORD IDord-d6214540b07f41f691e40f83b9cf0f40
Source noteuspto-grants-2003_07