HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,1,3-Benzothiadiazol-5-ylmethanol → 2,1,3-Benzothiadiazole-5-carbaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,1,3-Benzothiadiazol-5-ylmethanol | HCID 2776294 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 2,1,3-Benzothiadiazole-5-carbaldehyde | HCID 2776290 | 72.3% |
Reaction Steps
5-Hydroxymethylbenzo-2, 1,3-thiadiazole (2.6 g, 16 mmol) and manganese dioxide (6.0 g, 64 mmol) in chloroform (150 mL) were stirred at room temperature overnight. The reaction mixture was filtered off and the filtrate was evaporated to provide 1.9 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06593335B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-d6214540b07f41f691e40f83b9cf0f40 |
| Source note | uspto-grants-2003_07 |