Nitric Acid → HCID 18187089, compound

HRID 1357755Notes

Reaction equation

HRID 1357755 reaction equation
[F:1][CH:2]([F:12])[O:3][C:4]1[CH:11]=[CH:10][C:7]([CH:8]=[O:9])=[CH:6][CH:5]=1.[N+:13]([O-])([OH:15])=[O:14]>S(=O)(=O)(O)O>[F:1][CH:2]([F:12])[O:3][C:4]1[CH:5]=[CH:6][C:7]([CH:8]=[O:9])=[CH:10][C:11]=1[N+:13]([O-:15])=[O:14]

Participants

4

Reactant 2

HCID 944Nitric AcidHCID 2736986p-(Difluoromethoxy)benzaldehyde

Product 1

HCID 18187089HCID 18187089, compound

Reagents, catalysts & solvents 1

HCID 1118Sulfuric AcidSolvent

Procedure

10 4-Difluoromethoxybenzaldehyde (1.7 g, 10 mmol) was dissolved in concentrated sulfuric acid (8 mL) at 0 ° C. followed by dropwise addition of 70 % nitric acid (1,1 mL).

Sources & evidence

ORD record
ord-9a9e67143ed94d10bd014c28d3560feb
Source dataset
uspto-grants-2003_07
Patent number
US06593335B1

Reaction notes

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