HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → N-[4-(4-Benzotriazol-1-yl-piperidin-1-yl)-butyl]-3-pyridin-3-yl-acrylamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 3-(3-Pyridinyl)-2-propenoic acid | HCID 101984 | — |
| Reactant | 4-(4-Benzotriazol-1-yl-piperidin-1-yl)-butylamine | HCID 18187411 | — |
| Product | N-[4-(4-Benzotriazol-1-yl-piperidin-1-yl)-butyl]-3-pyridin-3-yl-acrylamide | HCID 53979662 | — |
Reaction Steps
Batch size: 3.1 g (22.5 mmol) 3-(3-pyridyl)-acrylic acid, 5.4 ml (45 mmol) oxalyl chloride and 5.6 g (20.5 mmol) 4-(4-benzotriazol-1-yl-piperidin-1-yl)-butylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06593344B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-61dfdcc5476e428a85d20457ec832d32 |
| Source note | uspto-grants-2003_07 |