HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanesulfonyl chloride → HCID 18184202, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanesulfonyl chloride | HCID 11667 | — |
| Reactant | HCID 18184222 | HCID 18184222 | — |
| Product | HCID 18184202 | HCID 18184202 | — |
Reaction Steps
According to the procedure described in Example 4a) 100 mg 5-isopropyl-N-[6-(2-aminoethoxy)-5-(o-methoxyphenoxy)-2-(4-pyridyl)-4-pyrimidinyl]-2-pyridine sulfonamide was reacted with ethanesulfonylchloride to give 83 mg 5-isopropyl-N-[6-(2-(ethanesulfonylamino)-ethoxy)-5-(o-methoxyphenoxy)-2-(2-pyridyl)-4-pyrimidinyl]-2-pyridine sulfonamide. LC-MS: tR=4.28 min, [M+1]+=629.63, [M−1]−=627.73.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06596719B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-8c7876482e9947fca3730b266df7dbc5 |
| Source note | uspto-grants-2003_07 |