HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 4-Hydrazinobenzenesulfonic acid morpholide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | 4-((4-Fluorophenyl)sulfonyl)morpholine | HCID 755377 | — |
| Solvent | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | 4-Hydrazinobenzenesulfonic acid morpholide | HCID 11299866 | — |
Reaction Conditions
| Temperature | 100 °C |
|---|
Reaction Steps
5 g of 4-fluorobenzenesulfonic acid morpholide were dissolved in 15 ml of N-methylpyrrolidone and mixed with 2.5 g of hydrazine hydrate, and the mixture was heated at 100° C. for 1 hour. After cooling to room temperature, 75 ml of water were added and the mixture was stirred at room temperature. After 2 hours, the solid was filtered off with suction and recrystallized from isopropanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06596742B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-32059fe74de94fbab9455921df158db1 |
| Source note | uspto-grants-2003_07 |