Ethanol → Ethyl (diphenylacetyl)carbamate

HRID 1358397Notes

Reaction equation

[C:1]1([CH:7]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[C:8]([N:10]=[C:11]=[O:12])=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH2:19]([OH:21])[CH3:20]>>[CH2:19]([O:21][C:11](=[O:12])[NH:10][C:8](=[O:9])[CH:7]([C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[CH3:20]

Participants

Reactant 2

HCID 702Ethanol

HCID 11264874Diphenylacetyl isocyanate

Product 1

HCID 9903898Ethyl (diphenylacetyl)carbamate

Procedure

The title compound, white solid, m.p. 133° C. and MS: m/e=284.2 (M+H+) was prepared in accordance with the general method of example 1 from diphenyl-acetyl isocyanate and ethanol.

Sources & evidence

ORD record: ord-4895190294d64c30bdf48597ace32493
Source dataset: uspto-grants-2003_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06596743B2

Reaction notes

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