3,4-Dimethoxyphenethyl alcohol → HCID 54573334, compound

HRID 1358403Notes

Reaction equation

[C:1]1([CH:7]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[C:8]([N:10]=[C:11]=[O:12])=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:19][O:20][C:21]1[CH:22]=[C:23]([CH2:29][CH2:30][OH:31])[CH:24]=[CH:25][C:26]=1[O:27][CH3:28]>>[CH3:19][O:20][C:21]1[CH:22]=[C:23]([CH2:29][CH2:30][O:31][C:11](=[O:12])[NH:10][C:8](=[O:9])[CH:7]([C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[CH:24]=[CH:25][C:26]=1[O:27][CH3:28]

Participants

Reactant 2

HCID 819113,4-Dimethoxyphenethyl alcohol

HCID 11264874Diphenylacetyl isocyanate

Product 1

HCID 54573334HCID 54573334, compound

Procedure

The title compound, white solid, m.p. 144° C. and MS: m/e=419.5 (M+H+) was prepared in accordance with the general method of example 1 from diphenylacetyl isocyanate and 2-(3,4-dimethoxy-phenyl)-ethanol.

Sources & evidence

ORD record: ord-4bbad09eb1874dfb9439c790155acf34
Source dataset: uspto-grants-2003_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06596743B2

Reaction notes

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