1-Butanol → HCID 53714410, compound

HRID 1358411Notes

Reaction equation

[C:1]1([C:7]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)([CH3:13])[C:8]([N:10]=[C:11]=[O:12])=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH2:20]([OH:24])[CH2:21][CH2:22][CH3:23]>>[CH2:20]([O:24][C:11](=[O:12])[NH:10][C:8](=[O:9])[C:7]([C:1]1[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1)([C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)[CH3:13])[CH2:21][CH2:22][CH3:23]

Participants

Reactant 2

HCID 2631-Butanol

HCID 22661083HCID 22661083, compound

Product 1

HCID 53714410HCID 53714410, compound

Procedure

The title compound, white solid, m.p.=83° C. and MS: m/e=325.4 (M+H+) was prepared in accordance with the general method of example 1 from 2,2-diphenylpropionyl isocyanate and butan-1-ol.

Sources & evidence

ORD record: ord-fb62d86c626b4d69b18b82bea1bf1646
Source dataset: uspto-grants-2003_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06596743B2

Reaction notes

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