2-Morpholinoethanol → HCID 54336575, compound

HRID 1358418Notes

Reaction equation

HRID 1358418 reaction equation
[C:1]1([CH:7]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[C:8]([N:10]=[C:11]=[O:12])=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[N:19]1([CH2:25][CH2:26][OH:27])[CH2:24][CH2:23][O:22][CH2:21][CH2:20]1>>[N:19]1([CH2:25][CH2:26][O:27][C:11](=[O:12])[NH:10][C:8](=[O:9])[CH:7]([C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[CH2:24][CH2:23][O:22][CH2:21][CH2:20]1

Participants

3

Reactant 2

HCID 611632-MorpholinoethanolHCID 11264874Diphenylacetyl isocyanate

Product 1

HCID 54336575HCID 54336575, compound

Procedure

The title compound, white solid, m.p.=135-137° C. and MS: m/e=369.3 (M+H−) was prepared in accordance with the general method of example 1 from diphenylacetyl isocyanate and 2-morpholin-4-yl-ethanol.

Sources & evidence

ORD record
ord-11b35e07a1494396bd2c8790b65364bf
Source dataset
uspto-grants-2003_07
Patent number
US06596743B2

Reaction notes

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