Carbamic acid, ethyl ester → HCID 57223634, compound

HRID 1358420Notes

Reaction equation

HRID 1358420 reaction equation
[F:1][C:2]([F:21])([F:20])[C:3]1[C:16]2[O:15][C:14]3[C:9](=[CH:10][CH:11]=[CH:12][CH:13]=3)[CH:8]([C:17](Cl)=[O:18])[C:7]=2[CH:6]=[CH:5][CH:4]=1.[CH2:22]([O:24][C:25](=[O:27])[NH2:26])[CH3:23]>>[CH2:22]([O:24][C:25](=[O:27])[NH:26][C:17]([CH:8]1[C:7]2[CH:6]=[CH:5][CH:4]=[C:3]([C:2]([F:21])([F:20])[F:1])[C:16]=2[O:15][C:14]2[C:9]1=[CH:10][CH:11]=[CH:12][CH:13]=2)=[O:18])[CH3:23]

Participants

3

Reactant 2

HCID 5641Carbamic acid, ethyl esterHCID 22661058HCID 22661058, compound

Product 1

HCID 57223634HCID 57223634, compound

Procedure

The title compound, white solid, m.p.=196-198° C., MS: m/e=365 (M+) was prepared in accordance with the general method of example 36 from 4-trifluoromethyl-9H-xanthene-9-carbonyl chloride and carbamic acid ethyl ester.

Sources & evidence

ORD record
ord-0be37f5957924d01855ce65d128cccf4
Source dataset
uspto-grants-2003_07
Patent number
US06596743B2

Reaction notes

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