9H-xanthene-9-carbonyl chloride → HCID 54046607, compound

HRID 1358447Notes

Reaction equation

HRID 1358447 reaction equation
[CH2:1]([C:4]1[O:8][C:7]([NH2:9])=[N:6][CH:5]=1)[CH2:2][CH3:3].[CH:10]1[C:23]2[CH:22]([C:24](Cl)=[O:25])[C:21]3[C:16](=[CH:17][CH:18]=[CH:19][CH:20]=3)[O:15][C:14]=2[CH:13]=[CH:12][CH:11]=1>>[CH2:1]([C:4]1[O:8][C:7]([NH:9][C:24]([CH:22]2[C:23]3[CH:10]=[CH:11][CH:12]=[CH:13][C:14]=3[O:15][C:16]3[C:21]2=[CH:20][CH:19]=[CH:18][CH:17]=3)=[O:25])=[N:6][CH:5]=1)[CH2:2][CH3:3]

Participants

3

Reactant 2

HCID 27608929H-xanthene-9-carbonyl chlorideHCID 226610715-Propyl-2-oxazolamine

Product 1

HCID 54046607HCID 54046607, compound

Procedure

The title compound, white solid, m.p. 203-205° C. and MS: m/e=334.1 (M+) was prepared in accordance with the general method of example 44a from 5-propyl-oxazol-2-ylamine [Ber. 95, 2419(1962)] and 9-xanthene-carboxylic acid chloride.

Sources & evidence

ORD record
ord-f8a6a427a8b64c33b41d2d064f382b26
Source dataset
uspto-grants-2003_07
Patent number
US06596743B2

Reaction notes

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