3-Phenylpropylamine → (3-Phenyl-n-propyl)aminosulfonylacetonitrile

HRID 1358723Notes

Reaction equation

HRID 1358723 reaction equation
[C:1]1([CH2:7][CH2:8][CH2:9][NH2:10])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:11]([CH2:13][S:14](Cl)(=[O:16])=[O:15])#[N:12].C(NS(CC#N)(=O)=O)C1C=CC=CC=1>>[C:1]1([CH2:7][CH2:8][CH2:9][NH:10][S:14]([CH2:13][C:11]#[N:12])(=[O:16])=[O:15])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

4

Reactant 3

HCID 162593-PhenylpropylamineHCID 13142426Cyanomethanesulfonyl chlorideHCID 15410493HCID 15410493, compound

Product 1

HCID 15410494(3-Phenyl-n-propyl)aminosulfonylacetonitrile

Procedure

N-3-Phenyl-n-propyl cyanomethylsulfonamide was prepared with 3-phenyl-n-propylamine and cyanomethylsulfonly chloride under similar conditions as described for N-benzyl cyanomethylsulfonamide (Part A, M40).

Sources & evidence

ORD record
ord-264ef813071e456283506e32069fa32f
Source dataset
uspto-grants-2003_07
Patent number
US06596878B2

Reaction notes

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