Sodium hydride → HCID 18185303, compound

Participants

Reaction Steps

N-(4-trifluoromethylthiobenzyl)benzamide (100 mg, 0.32 mmol) was coupled with 4-(trifluoromethylthio) benzyl bromide (91 mg, 0.34 mmol) using sodium hydride (9.2 mg, 0.38 mmol) to give 130 mg (80%) of N,N-bis(4-trifluoromethylthiobenzyl)benzamide as a yellow oil. 1HNMR (360 MHz, DMSO-d6) δ 7.65 (m, 4H), 7.31-7.47 (m, 9H), 4.57-4.66 (m, 4H). MS-EI m/z 501 [M+].

Provenance & Evidence