HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → 3,5-Bis-(2-nitro-4-trifluoromethanesulfonyl-phenoxy)-benzoic acid methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Methyl 3,5-Dihydroxybenzoate | HCID 75076 | — |
| Reactant | 1-Chloro-2-nitro-4-trifluoromethanesulfonylbenzene | HCID 1547956 | — |
| Product | 3,5-Bis-(2-nitro-4-trifluoromethanesulfonyl-phenoxy)-benzoic acid methyl ester | HCID 9917860 | — |
Reaction Steps
Using procedure as in example 10, a reaction of methyl 3,5-dihydroxybenzoate (50 mg, 0.297 mmol), NaH (26 mg, 2.2 equiv.) and 2-nitro-4-(trifluoromethylsulfonyl)chlorobenzene (172 mg, 0.595 mmol) afforded 3,5-bis-(2-nitro-4-trifluoromethanesulfonyl-phenoxy)-benzoic acid methyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06596772B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-58b213d0c9fc4ed689c562298d98f4ae |
| Source note | uspto-grants-2003_07 |