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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1358819Generated: November 1, 2026

HCID 69145286, compound → HCID 21876989, compound

https://huagongshe.com/reaction/1358819

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 69145286HCID 69145286—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 21876989HCID 2187698983.2%

Reaction Steps

A mixture of 4-[4-(3-phenylureido)benzyl]phenyl-carbamic acid benzyl ester (1.3 g) and 10% palladium on carbon (0.35 g) in ethanol (150 mL) was hydrogenated at 50 psi in a Parr apparatus for 12 hours. The reaction mixture filtered through a Celite pad to remove catalyst. The filtrate on concentration gave 4-[4-(3-phenylureido)benzyl]-phenylamine (0.76 g) as white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06596876B2
Source datasetuspto-grants-2003_07
ORD IDord-2ee56a8dc04845c1b7b50dd379ddbdfd
Source noteuspto-grants-2003_07