HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron → HCID 178427663, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron | HCID 5462311 | — |
| Reactant | HCID 178427660 | HCID 178427660 | — |
| Solvent | Ethyl orthoformate | HCID 31214 | — |
| Product | HCID 178427663 | HCID 178427663 | — |
Reaction Steps
A solution of N-hydroxy-N′-aminoguanidine tosylate (0.66 g; 2.5 mMol) in triethyl orthoformate (1.5 mL) in the presence of boron trifuloride etherate (10 mg) was stirred at room temperature during 8 h. The residue was filtered off and the product crystallised from the ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06599943B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-13378f0633194b70835b1aae09a31a83 |
| Source note | uspto-grants-2003_07 |