HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → 6-Bromo-1-[(dimethylamino)methyl]-2-naphthyl acetate hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | 6-Bromo-1-[(dimethylamino)methyl]-2-naphthol | HCID 14244482 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 6-Bromo-1-[(dimethylamino)methyl]-2-naphthyl acetate hydrochloride | HCID 69829662 | — |
Reaction Steps
6-Bromo-1-[(dimethylamino)methyl]-2-naphthol (5.6 g, 0.02 mol) was stirred in methylene chloride (120 mL). Acetyl chloride (3.0 mL, 0.042 mol) was added. The mixture was stirred at room temperature for 1 hour and the solvent was concentrated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06599925B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-eedb56077a364120afc35f98d228fe23 |
| Source note | uspto-grants-2003_07 |