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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1359265Generated: October 25, 2026

Hydrogen Bromide → HCID 178515992, compound

https://huagongshe.com/reaction/1359265

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrogen BromideHCID 260—
Reactant2-Benzyl-6-methoxypyridineHCID 21942274—
SolventWaterHCID 962—
ProductHCID 178515992HCID 17851599270.9%

Reaction Steps

A mixture of 59 g of 2-benzyl-6-methoxypyridine and 200 ml of 47% hydrobromic acid was heated under stirring for 7 hours in an oil bath kept at 100° C. After cooling as it was, 250 ml of water was added thereto, and the resulting crystals were collected by filtration, washed with water and vacuum-dried, to give 38.9 g of the target compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06599917B1
Source datasetuspto-grants-2003_07
ORD IDord-05486037a3b44e6cb1ec2598db258d0c
Source noteuspto-grants-2003_07