HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 15391440, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 15391431 | HCID 15391431 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 15391440 | HCID 15391440 | 71.4% |
Reaction Steps
0.38 g (1.0 mmol) of the nitro compound of Example 3 is reduced in 20 ml of methanol with RaNi and hydrazine hydrate analogously to Example 2. After boiling with ethanol, 0.25 g (71%) of the title compound of ethanol with a melting point of 280-289° C. (decomposition) is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06600036B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-16c1234b074840c4bb47796451b0912c |
| Source note | uspto-grants-2003_07 |