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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1359780Generated: November 1, 2026

Piperidine → HCID 59077522, compound

https://huagongshe.com/reaction/1359780

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPiperidineHCID 8082—
ReactantHCID 18179677HCID 18179677—
ReactantHCID 21139221HCID 21139221—
SolventEthanolHCID 702—
ProductHCID 59077522HCID 59077522—

Reaction Steps

A mixture of 5-phenylmethanesulfonyl-1,3-dihydro-indol-2-one (100 mg, 0.35 mmol), 3,5-dimethyl-4-(2-morpholin-4-yl-2-oxo-ethyl)-1H-pyrrole-2-carbaldehyde (166 mg, 0.68 mmol) and piperidine (0.5 eq.) in ethanol (2 mL) was stirred at rt for 48 hours. The reaction was concentrated and triturated with methanol to give the titled compound as a pale orange solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06599902B2
Source datasetuspto-grants-2003_07
ORD IDord-21428aed3e654f3d96271e024471e2ce
Source noteuspto-grants-2003_07