HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → HCID 59077522, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | HCID 18179677 | HCID 18179677 | — |
| Reactant | HCID 21139221 | HCID 21139221 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 59077522 | HCID 59077522 | — |
Reaction Steps
A mixture of 5-phenylmethanesulfonyl-1,3-dihydro-indol-2-one (100 mg, 0.35 mmol), 3,5-dimethyl-4-(2-morpholin-4-yl-2-oxo-ethyl)-1H-pyrrole-2-carbaldehyde (166 mg, 0.68 mmol) and piperidine (0.5 eq.) in ethanol (2 mL) was stirred at rt for 48 hours. The reaction was concentrated and triturated with methanol to give the titled compound as a pale orange solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06599902B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-21428aed3e654f3d96271e024471e2ce |
| Source note | uspto-grants-2003_07 |