Acetic Anhydride → HCID 59238262, compound

HRID 1359912Notes

Reaction equation

HRID 1359912 reaction equation
[C:1](OC(=O)C)(=[O:3])[CH3:2].[Br:8][C:9]1[CH:14]=[CH:13][C:12]([NH2:15])=[CH:11][C:10]=1[O:16][CH3:17]>C(O)(=O)C>[Br:8][C:9]1[CH:14]=[CH:13][C:12]([NH:15][C:1](=[O:3])[CH3:2])=[CH:11][C:10]=1[O:16][CH3:17]

Participants

4

Reactant 2

HCID 7918Acetic AnhydrideHCID 70182544-Bromo-3-methoxyaniline

Product 1

HCID 59238262HCID 59238262, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

Acetic anhydride (13 mL) is added to an ice-cold solution of 4-bromo-3-methoxy-phenylamine (25.0 g) in acetic acid (100 mL). The mixture is stirred for 1 h and then diluted with ice-cold water (500 mL). The precipitate is separated by filtration, washed with water and dried at 60° C. to give the product.

Workup

  1. customThe precipitate is separated by filtration
  2. washwashed with water
  3. customdried at 60° C.
  4. customto give the product

Sources & evidence

ORD record
ord-f25299f507ab442fb5cbc0dd8bbd45aa
Source dataset
uspto-grants-2011_02
Patent number
US07879806B2

Reaction notes

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