Aniline → HCID 24763214, compound

HRID 1360304Notes

Reaction equation

HRID 1360304 reaction equation
[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([O:24][CH3:25])=[C:6]([S:8]([N:11]2[C:16]3[CH:17]=[C:18]([C:21]([OH:23])=O)[CH:19]=[CH:20][C:15]=3[O:14][CH:13]=[CH:12]2)(=[O:10])=[O:9])[CH:7]=1.[NH2:26][C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1>>[C:27]1([NH:26][C:21]([C:18]2[CH:19]=[CH:20][C:15]3[O:14][CH:13]=[CH:12][N:11]([S:8]([C:6]4[CH:7]=[C:2]([Cl:1])[CH:3]=[CH:4][C:5]=4[O:24][CH3:25])(=[O:9])=[O:10])[C:16]=3[CH:17]=2)=[O:23])[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1

Participants

3

Reactant 2

HCID 6115AnilineHCID 66789329HCID 66789329, compound

Product 1

HCID 24763214HCID 24763214, compound

Procedure

Reaction of 4-(5-chloro-2-methoxy-benzenesulfonyl)-4H-benzo[1,4]oxazine-6-carboxylic acid with aniline in accordance with the general method of example 30, step 4 produced the title compound. Orange solid, MS (ISP)=455.2 (M−H)−.

Sources & evidence

ORD record
ord-678ac0edddf74f4e8ee204b93b17fa13
Source dataset
uspto-grants-2011_02
Patent number
US07879845B2

Reaction notes

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