HuagongsheHuagongshe Chemistry Print Report · For research reference only
(Z)-Benzaldehyde oxime → N-hydroxybenzenecarboximidoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (Z)-Benzaldehyde oxime | HCID 12143 | — |
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | N-hydroxybenzenecarboximidoyl chloride | HCID 2756315 | 93% |
Reaction Steps
α-Chlorobenzaldoxime was prepared according to the method described in Part A of Example 595 by reacting benzaldoxime (11.5 g, 94.9 mmol) in DMF (20 mL) with N-chlorosuccinimide (12.6 g, 94.9 mmol). α-Chlorobenzaldoxime (13.7 g, 93%) was obtained as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07879849B2 |
| Source dataset | uspto-grants-2011_02 |
| ORD ID | ord-5b6f3c70b422484c82fb977b2f743fef |
| Source note | uspto-grants-2011_02 |