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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1361216Generated: October 30, 2026

Hydrochloric Acid → HCID 66727315, compound

https://huagongshe.com/reaction/1361216

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
Reactant1,4-DioxaneHCID 31275—
ReactantHCID 66727467HCID 66727467—
SolventMethanolHCID 887—
ProductHCID 66727315HCID 66727315—

Reaction Steps

To a solution of 2-methyl-propane-2-sulfinic acid [(S)-1-(3-bromo-isoxazol-5-yl)-propyl]-amide (17.5 mg, 0.0566 mmol) in MeOH (1 mL) was added a 4 M solution of HCl in dioxane (0.70 mL, 0.28 mmol) dropwise. After 2.5 hours, the mixture was concentrated in vacuo to afford the title compound which was used with out purification. MS m/z 188.24 (M-53), 190.20 (M+2-53).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07879873B2
Source datasetuspto-grants-2011_02
ORD IDord-cf338a3166b74eb1b7ac01b55c01c7bd
Source noteuspto-grants-2011_02