HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Cyclohexen-1-one, 4,4-dimethyl- → Cyclohexanone, 4,4-dimethyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Cyclohexen-1-one, 4,4-dimethyl- | HCID 136839 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Pentane | HCID 8003 | — |
| Product | Cyclohexanone, 4,4-dimethyl- | HCID 138166 | 98.3% |
Reaction Steps
4,4-Dimethyl-cyclohexene-1-one (5 g, 40.3 mmol) and n-pentane (15 ml) were placed in a hydrogen reaction vessel, and Pd/C (500 mg) was added. The hydrogen reaction vessel was pressurized with hydrogen (25 psi), and reacted for 30 min. After the reaction finished, the reaction mixture was filtered through Celite, and the filtrate was concentrated in vacuo to give the title compound (5 g, 98%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07879852B2 |
| Source dataset | uspto-grants-2011_02 |
| ORD ID | ord-920d7992a32b47f3b93b993b10cb6af4 |
| Source note | uspto-grants-2011_02 |