HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl indole-2-carboxylate → Methyl N-methylindole-6-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl indole-2-carboxylate | HCID 73125 | — |
| Reactant | Methyl indole-6-carboxylate | HCID 639844 | — |
| Product | Methyl N-methylindole-6-carboxylate | HCID 639843 | 95% |
Reaction Steps
According to the procedure of Preparation 9 (a), except substituting methyl indole-6-carboxylate for the ethyl indole-2-carboxylate, the title compound (2.5 g, 95%) was obtained as white solid: MS (ES) m/e 190.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07879872B2 |
| Source dataset | uspto-grants-2011_02 |
| ORD ID | ord-60fd6428f8ee484eb83c59bade0f8833 |
| Source note | uspto-grants-2011_02 |