HRID1362848

反应详情

EQUATION

反应方程式

HRID 1362848 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A round-bottomed flask was charged with isatoic anhydride (5.0 g, 0.030 mol) and 30 mL water. Isopropylamine (4.64 mL, 0.049 mol) was added slowly to the reaction mixture. The product precipitated from the reaction mixture. After 1 h, the reaction mixture was filtered and washed with water to give 4.12 g (71% yield) of a white solid

WORKUP

后处理

  1. customThe product precipitated from the reaction mixture
  2. filtrationthe reaction mixture was filtered
  3. washwashed with water