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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1362973Generated: October 29, 2026

Triethylamine → HCID 46833681, compound

https://huagongshe.com/reaction/1362973

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethylamineHCID 8471—
Reactantm-Anisoyl chlorideHCID 74374—
Reactant4-(2-bromo-ethoxy)-3-(2-methyl-2H-pyrazol-3-yl)-phenylamineHCID 46833680—
SolventTetrahydrofuranHCID 8028—
ProductHCID 46833681HCID 4683368165.1%

Reaction Steps

A mixture of 4-(2-Bromoethoxy)-3-(2-methyl-2H-pyrazol-3-yl)-phenylamine (1.012 g, 3.417 mmole), 3-methoxy-benzoyl chloride (700 mg, 1.2 eq), and triethylamine (1.0 mL, 2 eq) in 5 mL THF was stirred at room temperature for 10 minutes. The mixture was purified by HPLC to give title compound as white solid (957 mg, 52%). Exact mass calculated for C20H20BrN3O3429.1. found 430.3 (M+H 79Br, 100), 432.5 (M+H 18Br, 98).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07884101B2
Source datasetuspto-grants-2011_02
ORD IDord-c94738aa762346488466490ea08deb89
Source noteuspto-grants-2011_02