Pyridinium chloride → HCID 66933837, compound

HRID 1363352Notes

Reaction equation

HRID 1363352 reaction equation
[OH:1][CH2:2][C@H:3]1[C@H:7]([C:8]2[C:9]([O:27]C)=[CH:10][C:11]([O:25]C)=[C:12]3[C:17]=2[O:16][C:15]([C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)=[CH:14][C:13]3=[O:24])[CH2:6][CH2:5][N:4]1[CH3:29].Cl.N1C=CC=CC=1>>[OH:25][C:11]1[CH:10]=[C:9]([OH:27])[C:8]([C@@H:7]2[CH2:6][CH2:5][N:4]([CH3:29])[C@H:3]2[CH2:2][OH:1])=[C:17]2[C:12]=1[C:13](=[O:24])[CH:14]=[C:15]([C:18]1[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=1)[O:16]2

Participants

3

Procedure

Compound of example 56 (0.5 g, 1.27 mmol) was treated with dry pyridine hydrochloride (5 g, 43.29 mmol) as described in the example 17, to obtain the title compound.

Sources & evidence

ORD record
ord-dfdc9e70e20641139caf341809bafd75
Source dataset
uspto-grants-2011_02
Patent number
US07884127B2

Reaction notes

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