Pyridinium chloride → HCID 66933837, compound
Reaction equation
[OH:1][CH2:2][C@H:3]1[C@H:7]([C:8]2[C:9]([O:27]C)=[CH:10][C:11]([O:25]C)=[C:12]3[C:17]=2[O:16][C:15]([C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)=[CH:14][C:13]3=[O:24])[CH2:6][CH2:5][N:4]1[CH3:29].Cl.N1C=CC=CC=1>>[OH:25][C:11]1[CH:10]=[C:9]([OH:27])[C:8]([C@@H:7]2[CH2:6][CH2:5][N:4]([CH3:29])[C@H:3]2[CH2:2][OH:1])=[C:17]2[C:12]=1[C:13](=[O:24])[CH:14]=[C:15]([C:18]1[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=1)[O:16]2Participants
3
Procedure
Compound of example 56 (0.5 g, 1.27 mmol) was treated with dry pyridine hydrochloride (5 g, 43.29 mmol) as described in the example 17, to obtain the title compound.
Sources & evidence
- ORD record
- ord-dfdc9e70e20641139caf341809bafd75
- Source dataset
- uspto-grants-2011_02
- Patent number
- US07884127B2
Reaction notes
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