Pyridinium chloride → HCID 131728672, compound

HRID 1363377Notes

Reaction equation

HRID 1363377 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8]1[O:9][C:10]2[C:15]([C:16](=[O:18])[CH:17]=1)=[C:14]([O:19]C)[CH:13]=[C:12]([O:21]C)[C:11]=2[C@@H:23]1[CH2:27][CH2:26][N:25]([CH3:28])[C@H:24]1[CH2:29][N:30]1[CH:34]=[CH:33][N:32]=[CH:31]1.Cl.N1C=CC=CC=1>>[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8]1[O:9][C:10]2[C:15]([C:16](=[O:18])[CH:17]=1)=[C:14]([OH:19])[CH:13]=[C:12]([OH:21])[C:11]=2[C@@H:23]1[CH2:27][CH2:26][N:25]([CH3:28])[C@H:24]1[CH2:29][N:30]1[CH:34]=[CH:33][N:32]=[CH:31]1

Participants

3

Reactant 2

HCID 10176127Pyridinium chlorideHCID 131728673HCID 131728673, compound

Product 1

HCID 131728672HCID 131728672, compound

Procedure

A mixture of compound of example 112 (0.3 g, 0.625 mmol) and pyridine hydrochloride (3.0 g, 26.0 mmol) was heated as described in example 17 to get the title compound.

Workup

  1. temperaturewas heated

Sources & evidence

ORD record
ord-2e9eb3bc62d4409597ec256c604879de
Source dataset
uspto-grants-2011_02
Patent number
US07884127B2

Reaction notes

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