Sodium Hydroxide → HCID 131728684, compound

HRID 1363392Notes

Reaction equation

HRID 1363392 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8]1[O:9][C:10]2[C:15]([C:16](=[O:18])[CH:17]=1)=[C:14]([O:19][CH3:20])[CH:13]=[C:12]([O:21][CH3:22])[C:11]=2[C@@H:23]1[CH2:27][CH2:26][N:25]([CH2:28][CH2:29][CH3:30])[C@H:24]1[CH2:31][O:32]C(=O)C.[OH-].[Na+]>CO>[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8]1[O:9][C:10]2[C:15]([C:16](=[O:18])[CH:17]=1)=[C:14]([O:19][CH3:20])[CH:13]=[C:12]([O:21][CH3:22])[C:11]=2[C@@H:23]1[CH2:27][CH2:26][N:25]([CH2:28][CH2:29][CH3:30])[C@H:24]1[CH2:31][OH:32]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 131728685HCID 131728685, compound

Product 1

HCID 131728684HCID 131728684, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Compound of example 130 (0.2 g, 0.04 mmol) in methanol (5 mL) was subjected to hydrolysis using a 10% NaOH solution (5 mL) according to the procedure in example 4 to get the title compound.

Sources & evidence

ORD record
ord-52222df1b709487caf5d52e6dd5e5ee4
Source dataset
uspto-grants-2011_02
Patent number
US07884127B2

Reaction notes

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