Sodium Carbonate → HCID 66933619, compound

Participants

Reaction Steps

Compound of example 41 (0.3 g, 0.6 mmol) was treated with iron dust (0.3 g) in water (1.2 mL) and glacial acetic acid (1.2 mL). The reaction mixture was stirred vigorously at room temperature for 1 h. It was poured into water (25 mL), basified using saturated aqueous Na2CO3 solution and extracted with EtOAc (3×25 mL). The organic extract was washed, dried (anhydrous Na2SO4) and concentrated to obtain the title compound.

Provenance & Evidence