Sodium Carbonate → HCID 178428275, compound

HRID 1363855Notes

Reaction equation

HRID 1363855 reaction equation
Cl.[Cl-].[NH2:3][C:4]1[C:5]([NH:13][CH2:14][CH2:15][N+:16]([CH3:19])([CH3:18])[CH3:17])=[N:6][N:7]2[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=12.[NH2:20][C:21]1[C:22]([Cl:29])=[C:23]([OH:28])[C:24]([CH3:27])=[CH:25][CH:26]=1.C(=O)([O-])[O-].[Na+].[Na+]>O>[Cl-:29].[NH2:20][C:21]1/[C:26](=[N:3]/[C:4]2[C:5]([NH:13][CH2:14][CH2:15][N+:16]([CH3:19])([CH3:18])[CH3:17])=[N:6][N:7]3[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=23)/[CH:25]=[C:24]([CH3:27])[C:23](=[O:28])[C:22]=1[Cl:29]

Participants

5

Reactant 3

HCID 10340Sodium CarbonateHCID 1576415-Amino-6-Chloro-o-CresolHCID 66923186HCID 66923186, compound

Product 1

HCID 178428275HCID 178428275, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

5.83 mmol of 2-[(3-aminopyrazolo[1,5-a]pyridin-2-yl)amino]-N,N,N-trimethylethanaminium chloride hydrochloride dissolved in 30 ml of water were placed in a 100 ml one-necked round-bottomed flask. 5.83 mmol of 3-amino-2-chloro-6-methylphenol and then 17.5 mmol of sodium carbonate were added to this solution.

Workup

  1. customwere placed in a 100 ml one-necked round-bottomed flask

Sources & evidence

ORD record
ord-6d0ad1c1ca8d46d7951b8599a4dc527c
Source dataset
uspto-grants-2011_02
Patent number
US07887601B2

Reaction notes

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