HRID1363956

反应详情

EQUATION

反应方程式

HRID 1363956 的结构方程式

PROCEDURE

实验过程

Phenyl chloroformate (6.2 g, 40.2 mmol) was added to a solution of tert-butyl 4-(prop-2-ynyl)piperidine-1-carboxylate (1.65 g, 13.4 mmol) according to general procedure 1. Yield=0.600 g, 34%. m/z MH+=244.08. HPLC rt=10.3 min.

WORKUP

后处理

  1. customHPLC rt=10.3 min.