HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Dimethylaniline → HCID 57838883, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Dimethylaniline | HCID 949 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | 3-Nitrophenol | HCID 11137 | — |
| Reactant | Triphosgene | HCID 94429 | — |
| Product | HCID 57838883 | HCID 57838883 | — |
Reaction Steps
3-Nitrophenol (4.12 g, 29.6 mmol) was added as a solution in THF and dimethylaniline to a mixture of triphosgene (2.849 g, 9.6 mmol) in THF according to general procedure 3. Yield=5.53 g, 86%. m/z MH+=289.18. HPLC rt=11.78 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07888329B2 |
| Source dataset | uspto-grants-2011_02 |
| ORD ID | ord-5badfbf5055f4e14b56641a8bffee870 |
| Source note | uspto-grants-2011_02 |