HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → (2,5-Dimethoxyphenyl)acetyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 2,5-Dimethoxyphenylacetic acid | HCID 74469 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | (2,5-Dimethoxyphenyl)acetyl chloride | HCID 596088 | — |
Reaction Steps
To a solution of 196 mg (1.00 mmol) of (2,5-dimethoxyphenyl)acetic acid in 3 mL of CH2Cl2 was added 100 μL of oxalyl chloride. The mixture was stirred at ambient temperature for 1 hour then concentrated under reduced pressure to a thick liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07888374B2 |
| Source dataset | uspto-grants-2011_02 |
| ORD ID | ord-5f39d295ad2548daab8b070d6410a14a |
| Source note | uspto-grants-2011_02 |