HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methyl-2H-pyrazol-3-ylamine → HCID 58614747, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methyl-2H-pyrazol-3-ylamine | HCID 136927 | — |
| Reactant | 3-Chloro-4-(4-chloro-3-(pyridin-2-yl)phenylcarbamoyl)benzoic acid | HCID 66878605 | — |
| Product | HCID 58614747 | HCID 58614747 | — |
Reaction Steps
50 mg of 3-chloro-4-(4-chloro-3-(pyridin-2-yl)phenylcarbamoyl)benzoic acid was coupled to 5-amino-1-methylpyrazole via Procedure G. The product was purified on reverse phase HPLC to yield 2-chloro-N1-(4-chloro-3-(pyridin-2-yl)phenyl)-N4-(1-methyl-1H-pyrazol-5-yl)terephthalamide. MS (Q1) 466 (M)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07888364B2 |
| Source dataset | uspto-grants-2011_02 |
| ORD ID | ord-340e18c0a47f4c30a06eee2a8138e223 |
| Source note | uspto-grants-2011_02 |