HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Pyrrolidin-2-yl)ethan-1-amine → HCID 178512125, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Pyrrolidin-2-yl)ethan-1-amine | HCID 14030009 | — |
| Reactant | HCID 66877087 | HCID 66877087 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178512125 | HCID 178512125 | — |
Reaction Steps
Ethyl 4-(4-chloro-3-(pyridin-2-yl)phenylcarbamoyl)benzimidate (2.0 ml of a 0.075 M methanol solution, 0.15 mmol) was treated with 2-(pyrrolidin-2-yl)ethanamine (28 μl, 0.23 mmol) via procedure W to afford 90 mg of N-(4-chloro-3-(pyridin-2-yl)phenyl)-4-(N-(2-(pyrrolidin-2-yl)ethyl)carbamimidoyl)benzamide. MS (Q1) 448 (M)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07888364B2 |
| Source dataset | uspto-grants-2011_02 |
| ORD ID | ord-0aa5604155a14eb5a21da30dedf9118b |
| Source note | uspto-grants-2011_02 |