HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanolamine → 2-Benzamidoethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | Methyl Benzoate | HCID 7150 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2-Benzamidoethanol | HCID 569526 | 11% |
Reaction Steps
Under an argon atmosphere, a mixture of methyl benzoate (3.0 mmol), 2-aminoethanol (3.6 mmol), Zn4(OCOCF3)6O (0.15 mmol) and methylene chloride (2.5 mL) was stirred at room temperature for 3 days, and as a result, N-(2-hydroxyethyl)benzamide was obtained in 11% yield. The resulting compound was identified by comparison with physical property data of the known compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07888513B2 |
| Source dataset | uspto-grants-2011_02 |
| ORD ID | ord-a663e7c8c7dd41ad88739b85d439c8fd |
| Source note | uspto-grants-2011_02 |