HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetraethoxysilane → HCID 86643014, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetraethoxysilane | HCID 6517 | — |
| Reactant | 1-Butanaminium, N,N,N-trimethyl-, hydroxide (1:1) | HCID 45658 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86643014 | HCID 86643014 | — |
Reaction Steps
Trimethylbutylammonium hydroxide, (25.66%), 366.4 g, was diluted with 564.8 g deionized water and to it there were added 500.0 g of tetraethylorthosilicate, (98%) with stirring. After hydrolysis was complete, the solution was placed on a rotary evaporator to remove the alcohol. Elemental analysis showed the solution to contain 7.04 wt % Si.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07888544B2 |
| Source dataset | uspto-grants-2011_02 |
| ORD ID | ord-75f34e35aad24f428753949f1ab75fee |
| Source note | uspto-grants-2011_02 |