HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylmorpholine → (R)-2-AMino-N,N-diMethylpropanaMide HCl
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylmorpholine | HCID 7972 | — |
| Reactant | Dimethylamine, hydrochloride | HCID 10473 | — |
| Reactant | N-Cbz-d-alanine | HCID 70832 | — |
| Product | (R)-2-AMino-N,N-diMethylpropanaMide HCl | HCID 57516590 | — |
Reaction Steps
N1,N1-dimethyl-D-alaninamide, hydrochloride salt was prepared in a manner similar to Example 69, utilizing N-CBZ-D-alanine in place of N-CBZ-glycine, utilizing dimethylamine, hydrochloride salt in place of pyrrolidine, and using 3 equivalents of NMM.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07893056B2 |
| Source dataset | uspto-grants-2011_02 |
| ORD ID | ord-ac3e030a4e9e40b5b529adbc944b5917 |
| Source note | uspto-grants-2011_02 |