HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 66936184, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 66936465 | HCID 66936465 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 66936184 | HCID 66936184 | 112.2% |
Reaction Steps
1-(Diphenylmethyl)-3-ethyl-N,N-dimethyl-3-azetidinamine (0.215 g, 0.73 mmol) in 1 N HCl (5 ml) and ethanol (30 ml) was treated with H2 at 60 psi in the presence of Pd(OH)2 on carbon (100 mg). Standard work-up afforded 3-ethyl-N,N-dimethyl-3-azetidinamine dihydrochloride (0.165 g, 112.2%). LCMS: (M+H)+ 129.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07893056B2 |
| Source dataset | uspto-grants-2011_02 |
| ORD ID | ord-6719398001474402b98b0310cc89becd |
| Source note | uspto-grants-2011_02 |