Phosphorus oxychloride → HCID 57718206, compound

Participants

Reaction Steps

A solution of 10 (150 mg, 0.26 mmol) in POCl3 (0.24 mL, 2.6 mmol) was heated to 90° C. for 3.5 hours. The mixture was cooled to room temperature and poured onto ice. The precipitate was collected by filtration, washed with water and dried under vacuum to afford 11 as a pale yellow solid (143 mg), which was used without further purification. Mass Spectrum m/e=594.8 (M+1)

Provenance & Evidence