HRID1366958

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID96598

1H-Pyrrole-2-carboxylic acid, 5-methyl-, ethyl ester

C8H11NO2

HCID2760403

2-phenylpropanoyl chloride

C9H9ClO

PRODUCTS

生成物

结构：CCOC(=O)c1cc(C(=O)C(C)c2ccccc2)c(C)[nH]1

HCID57435143

未命名化合物

PROCEDURE

实验过程

5-Methyl-4-(2-phenyl-propionyl)-1H-pyrrole-2-carboxylic acid ethyl ester (138) was synthesized from 5-methyl-1H-pyrrole-2-carboxylic acid ethyl ester (107) and 2-phenyl-propionyl chloride following the procedure described in Example 32. Reaction conditions: 1,2-dichloromethane/−40° C.→RT. Purification: no purification. LC/MS: 86%.

WORKUP

后处理

customReaction conditions
customPurification
customno purification