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HRID1366959

反应详情

EQUATION

反应方程式

HRID 1366959 的结构方程式

REACTANTS

反应物

2
结构：CCOC(=O)c1ccc[nH]1
HCID255670

Ethyl pyrrole-2-carboxylate

C7H9NO2

结构：O=C(Cl)Cc1ccc2ccccc2c1
HCID588115

2-(2-NAPHTHYL)ACETYL CHLORIDE

C12H9ClO

PRODUCTS

生成物

1
结构：CCOC(=O)c1cc(C(=O)Cc2ccc3ccccc3c2)c[nH]1
HCID57435146

未命名化合物

PROCEDURE

实验过程

4-(2-Naphthalen-2-yl-acetyl)-1H-pyrrole-2-carboxylic acid ethyl ester (141) was synthesized from 1H-pyrrole-2-carboxylic acid ethyl ester and naphthalen-2-yl-acetyl chloride following the procedure described in Example 32. Reaction Conditions: 1,2-dichloromethane/−40° C.→RT. Purification: no purification. LC/MS: 78%.

WORKUP

后处理

  1. customReaction Conditions
  2. customPurification
  3. customno purification